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<解説編>本書におけるデータ測定法 <データ編>収録データ項目:材料名/構造式/HOMO/LUMO/吸収端波長/PLピーク波長/PL量子収率/蛍光寿命/吸収・発光・励起スペクトル/イオン化ポテンシャル/膜厚/有機半導体/有機EL/光学物性/電子物性/仕事関数/イオン化ポテンシャル/蛍光寿命/量子収率
刊行にあたって
π電子系からなる有機薄膜は、その分子構造に依存して、多彩な電子的、光学的性質を示すことが、過去25年間の研究開発で明らかにされてきた。1980年代後半、有機化合物からなる100nm程度の超薄膜に10V程度の電圧を印加すると、本来絶縁体であった有機薄膜が、～1A/cm2に達する大電流を流し、あたかも半導体の様に振る舞うことが確認された。実は、この当時、研究者たちは、それほど、事の重大性には気がついていなかったと思われるが、実は、有機薄膜において絶縁体から導電体への大きなパラダイムシフトが起きた瞬間であった。その後、様々な薄膜パラメーターの最適化や光・電子物性の解明が進み、急速に、有機半導体エレクトロニクスが確立されてきた。特に、有機ELデバイスは、なかでも特記すべきフラッグシップデバイスであり、電極からのキャリヤー注入、有機層内でのキャリヤー輸送、キャリヤー再結合、そして、励起子失活(発光)と多彩な電子過程を経由して発光に至る。この有機ELの研究開発過程において、包括的に有機半導体材料が世界規模で合成され、その数はたぶん10万点を超えると予想される。九州大学安達研究室においても、過去25年間で、約1400種類の有機半導体材料を合成してきた。今回、保有材料から113点を選び、その薄膜の基礎的な光学物性、電子物性を計測し、データ集としてとりまとめた。これらのデータが、今後の有機半導体材料の開発に少しでもお役に立てれば幸いである。
最後に、本データ集を編纂するにあたり、根気よくデータを測定、整理して頂いた安達研テクニカルスタッフのみなさんに深く感謝致します。また、一部貴重な材料をご提供頂いた関係者の皆様にもこの場を借りて深く感謝致します。
2012年9月 安達千波矢
著者一覧
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【 解説編】
<本書におけるデータ測定法>
1 大気中光電子分光装置
1.1 測定結果の解析
2 絶対PL量子収率測定装置
3 小型蛍光寿命測定装置
【 データ編】
データの補足説明
データ一覧
材料別に以下のデータを収録。
・構造式
・HOMO/LUMO
・吸収端波長
・PLピーク波長
・PL量子収率
・蛍光寿命(測定値および計測図)
・吸収・発光・励起スペクトル計測図
・イオン化ポテンシャル計測図
・膜厚
(収録材料名一覧)
1,1'-[1,1'-Biphenyl]-4,4'-diylbis[3,6,8-tris(3-methylphenyl)-pyrene (9CI)
1,1-Bis[4-(N-biphenylyl-N-phenylamino)phenyl]cyclohexane
1,1-Bis[4-[N,N’-di(biphenylyl)amino]phenyl]cyclohexane
1,1-Bis[4-[N,N'-di(p-tolyl)amino]-phenyl]cyclohexane
1,3,5-Tris(1-phenyl-1H-benzo[d]imidazol-2-yl)benzene
1,3,6,8-Tetra([1,1'-biphenyl]-3-yl)-pyrene
1,3,6,8-Tetra(3-biphenylyl)pyrene1,3,6,8-Tetra(4-biphenylyl)pyrene
1,3,6,8-Tetra(4-trifluoromethyl-phenyl)pyrene
1,3,6,8-Tetrastyrylpyrene
1,3,6-Tri(m-tolyl)pyrene1,3-Bis(N-carbazolyl)benzene
1,3-Bis[2-(2,2'-bipyridine-6-yl)-1,3,4-oxadiazol-5-yl]benzene
1,4-Bis(2,2-diphenylvinyl)benzene
1,4-Bis(3,5-(9-dicarbazolyl)styryl)benzene
1,4-Bis(4-(hexyloxy)styryl)benzene
1,4-Bis(4-methylstyryl)benzene1,4-Bis(4-octylstyryl)benzene
1,4-Bis(p-(N-phenyl-N-(m-tolyl)amino)styryl)benzene
1,4-Bis(triphenylsilyl)benzene
1,4-Bis[1-(3,6,8-triphenyl)pyrenyl]benzene
1,4-Bisstyrylbenzene
1,6-Bis(2-(4-hexylphenyl)ethynyl)pyrene
1,6-Bis(4-(4-butylstyryl)phenyl)pyrene
1,6-Bis(4-butylstyryl)pyrene1,6-Bis(4-octylstyryl)pyrene
1,6-Bis(4-propylstyryl)pyrene
1,6-Bis[2-(4-ethylphenyl)ethenyl]pyrene
1,8-Bis(4-hexylstyryl)pyrene
1,8-Bis(p-hexylphenylethynyl)pyrene
(1E)-1,2-Bis(4-styrylphenyl)ethene
1-((E)-2-(Pyren-3-yl)vinyl)-4-((E)-2-(pyren-8-yl)vinyl)benzene
2,3,6,7-Tetra(2-naphthyl)naphthalene
2,3,6,7-Tetra(4-biphenylyl)naphthalene
2,3,6,7-Tetraphenylnaphthalene2,3,6,7-Tetrastyrylnaphthalene
2-(4-Biphenyl)-5-(4-tert-butyl-phenyl)-1,3,4-oxadiazole
2,7-Bis(2-(4-hexylphenyl)ethynyl)pyrene
2,7-Bis(4-octylstyryl)-9,9-dimethyl-9H-fluorene
2,7-Bis(4-(trifluoromethyl)phenyl)pyrene
2,7-Bis(6-hexyl-2-naphthaleyl)-pyrene
2,9-Dimethyl-4,7-diphenyl-1,10-phenanthroline
2-(9H-Carbazol-9-yl)-5-[4'-(9H-carbazol-9-yl)-1,1'-biphenyl-4-yl]-pyridine
2-Methyl-9,10-bis(naphthalen-2-yl)anthracene
2-tert-Butyl-9,10-bis(2-naphthyl)anthracene
3,3’,5,5’-Tetraphenyl-p-terphenyl
4-(2,2-Diphenylethenyl)-N,N-bis(4-methylphenyl)Benzenamine
4,4''-(1,2-Ethenediyl)bis[4'-(butyl)-1,1'-biphenyl]
4,4''-(1,2-Ethenediyl)bis[4'-trifluoromethyl-1,1'-biphenyl]
4,4'-(1,2-Ethenediyl)bisbenzonitrile
4,4''-[1,4-Phenylenedi-(1E)-1,2-ethenediyl]bis[4'-trifluoromethyl-1,1'-biphenyl
4,4''-[1,4-Phenylenedi-(1E)-2,1-ethenediyl]bis[4'-pentyl-1,1'-bi-phenyl]
4,4'-(1,4-Phenylenedi-2,1-ethenediyl)bisbenzonitrile
4,4',4''-Tris(N-3-methylphenyl-N-phenylamino)triphenylamine
4,4’-Bis[1-(3,6,8-triphenyl)pyrenyl]biphenyl
4,4'-Bis[(1E)-2-[4'-(trifluoromet-hyl)[1,1'-biphenyl]-4-yl]ethenyl]-1,1'-biphenyl
4,4'-Bis[2-(4'-butyl[1,1'-biphenyl]-4-yl)ethenyl]-1,1'-biphenyl
4,4'-Bis[2-(4-cyclohexylphenyl)ethenyl]-1,1'-biphenyl
4,4'-Bis[2-(4-decylphenyl)ethenyl]-1,1'-biphenyl
4,4'-Bis[2-(4-dodecylphenyl)ethenyl]-1,1'-biphenyl
4,4''-Bis[2-(4-hexylphenyl)ethenyl]-1,1':4',1''-terphenyl
4,4'-Bis[2-[4-(octyloxy)phenyl]ethenyl]-1,1'-biphenyl
4,4''-Bis[2-(4-octylphenyl)ethenyl]-1,1':4',1''-terphenyl
4,4'-Bis[2-(4-octylphenyl)ethenyl]-1,1'-biphenyl
4,4''-Bis[2-(4-pentylphenyl)ethenyl]-1,1':4',1''-terphenyl
4,4'-Bis[2-(4-pentylphenyl)ethenyl]-1,1'-biphenyl
4,4'-Bis[4-(di-p-tolylamino)styryl]biphenyl
4,4'-Bis(4'-n-heptyl-4-biphenylyl)-stilbene (7CI)
4,4'-Bis(9-carbazolyl)-2,2'-dimeth-ylbiphenyl
4,4’-Bis[di(m-tolyl)amino]terphenyl
4,4’-Bis(diphenylamino)terphenyl
4',4''-Bis[di(p-tert-butylphenyl)amino]-p-terphenyl
4,4'-Bis(N-carbazolyl)-1,1'-biphenyl
4,7-Diphenyl-1,10-phenanthroline
5,5'-Bis[1-(3,6,8-triphenyl)pyrenyl]-2,2'-bipydine
7,7'-Spirobi[7H-dinaphtho[2,1-b:1',2'-d]silole] (9CI)
7,12-Diphenylbenzo[k]fluoranthene
9-(3-(4-(3,5-Bis(9H-carbazol-9-yl)styryl)styryl)-5-(9H-carbazol-9-yl)phenyl)-9H-carbazole
9-(4-(4-(4-(9H-Carbazol-9-yl)styryl)styryl)phenyl)-9H-carbazole
9,9'-[[1,1'-Biphenyl]-4,4'-diylbis-(2,1-ethenediyl-3,1-phenylene)]bis-9H-carbazole
9,9'-(1,6-Pyrenediyldi-4,1-phenylene)bis-9H-Carbazole
9,9'-(2,6-Pyridinediyl)bis-9H-carbazole
9,9',9'',9'''-[[1,1'-Biphenyl]-4,4'-diylbis(2,1-ethenediyl-5,1,3-benzenetriyl)]tetrakis-9H-carbazole
9,9'-Biphenyl-3,3'-diylbis-9H-carbazole
9,9-Bis[4-[N,N'-di(4-biphenylyl)amino]phenyl]fluorene
9,10-Bis([1,1'-biphenyl]-3-yl)anthracene
9,10-Diphenylanthracene
a,a'-(1,4-Phenylenedimethylidyne)bis-4-ethyl-benzeneacetonitrile
a,a'-Bis(4-ethyl-phenylmethylene)-1,4-benzenediacetonitrile
Bis[2-(diphenylphosphino)phenyl]ether oxide
Cupper(II) phthalocyanine
Dioctylbenzothieno[2,3-b]benzothiophene
Dipyrazino[2,3-f:2',3'-h]quinoxaline-2,3,6,7,10,11-hexacarbonitrile
Fullerene C60
N4-[4'-(Diphenylamino)-[3,3'-dimethyl-1,1'-biphenyl]-4-yl]-N4,N4',N4'-triphenyl-[3,3'-dime-thyl-1,1'-biphenyl]-4,4'-diamine
N4,N4''-(9H-Fluoren-9-ylidenedi-4,1-phenylene)bis[N4,N4',N4'-triphenyl-[1,1'-biphenyl]-4,4'-diamine]
N4,N4'-Bis[4'-([1,1'-biphenyl]-3-ylphenylamino)[1,1'-biphenyl]-4-yl]-N4,N4'-diphenyl-[1,1'-biphenyl]-4,4'-diamine
N4,N4'-Bis[4'-[(4-tert-butylphenyl)phenylamino][1,1'-biphenyl]-4-yl]-N4,N4'-diphenyl[1,1'-biphenyl]-4,4'-diamine
N4,N4'-(Biphenyl-4,4'-diyl)bis(N4,N4',N4'-triphenylbiphenyl-4,4'diamine)
N4,N4''-Bis[4'-(diphenylamino)[1,1'-biphenyl]-4-yl]-N4,N4''-diphenyl-[1,1':4',1''-terphenyl]-4,4''-diamine
N4,N4''-(Cyclohexylidenedi-4,1-phenylene)bis[N4,N4',N4'-triphenyl-[1,1'-biphenyl]-4,4'-diamine]
N4,N4,N4',N4'-Tetra([1,1'-biphenyl]-3-yl)[1,1'-biphenyl]-4,4'-diamine
Naphtho[2,3-b]naphtho[2',3':4,5]thieno[2,3-d]thiophene
N,N'-Bis(3-methylphenyl)-N',N'-bis(phenyl)-benzidine
N,N'-Bis[4'-([1,1'-biphenyl]-4-yl-phenylamino)[1,1'-biphenyl]-4-yl]-N,N'-diphenyl[1,1':4',1''-terphenyl]-4,4''-diamine
N,N-Bis[4'-(diphenylamino)[1,1'-biphenyl]-4-yl]-N',N'-diphenyl-[1,1'-biphenyl]-4,4'-diamine
N,N'-Bis[4'-(diphenylamino)[1,1'-biphenyl-4yl]-N,N'diphenyl-[3-phenyl-1,1'-biphenyl]-4,4'-diamine
N,N'-Di(1-naphthyl)-N,N'-diphenylbenzidine
N,N'-Diphenyl-N,N'-di-[4-(N,N-ditolyl-amino)phenyl]benzidine
N,N,N',N'-Tetra(4-biphenylyl)benzidine
PentacenePhenyl-dipyreylphosphine oxide
Tris(8-hydroxyquinolinato)aluminium
略称材料名索引
<本書におけるデータ測定法>
1 大気中光電子分光装置
1.1 測定結果の解析
2 絶対PL量子収率測定装置
3 小型蛍光寿命測定装置
【 データ編】
データの補足説明
データ一覧
材料別に以下のデータを収録。
・構造式
・HOMO/LUMO
・吸収端波長
・PLピーク波長
・PL量子収率
・蛍光寿命(測定値および計測図)
・吸収・発光・励起スペクトル計測図
・イオン化ポテンシャル計測図
・膜厚
(収録材料名一覧)
1,1'-[1,1'-Biphenyl]-4,4'-diylbis[3,6,8-tris(3-methylphenyl)-pyrene (9CI)
1,1-Bis[4-(N-biphenylyl-N-phenylamino)phenyl]cyclohexane
1,1-Bis[4-[N,N’-di(biphenylyl)amino]phenyl]cyclohexane
1,1-Bis[4-[N,N'-di(p-tolyl)amino]-phenyl]cyclohexane
1,3,5-Tris(1-phenyl-1H-benzo[d]imidazol-2-yl)benzene
1,3,6,8-Tetra([1,1'-biphenyl]-3-yl)-pyrene
1,3,6,8-Tetra(3-biphenylyl)pyrene1,3,6,8-Tetra(4-biphenylyl)pyrene
1,3,6,8-Tetra(4-trifluoromethyl-phenyl)pyrene
1,3,6,8-Tetrastyrylpyrene
1,3,6-Tri(m-tolyl)pyrene1,3-Bis(N-carbazolyl)benzene
1,3-Bis[2-(2,2'-bipyridine-6-yl)-1,3,4-oxadiazol-5-yl]benzene
1,4-Bis(2,2-diphenylvinyl)benzene
1,4-Bis(3,5-(9-dicarbazolyl)styryl)benzene
1,4-Bis(4-(hexyloxy)styryl)benzene
1,4-Bis(4-methylstyryl)benzene1,4-Bis(4-octylstyryl)benzene
1,4-Bis(p-(N-phenyl-N-(m-tolyl)amino)styryl)benzene
1,4-Bis(triphenylsilyl)benzene
1,4-Bis[1-(3,6,8-triphenyl)pyrenyl]benzene
1,4-Bisstyrylbenzene
1,6-Bis(2-(4-hexylphenyl)ethynyl)pyrene
1,6-Bis(4-(4-butylstyryl)phenyl)pyrene
1,6-Bis(4-butylstyryl)pyrene1,6-Bis(4-octylstyryl)pyrene
1,6-Bis(4-propylstyryl)pyrene
1,6-Bis[2-(4-ethylphenyl)ethenyl]pyrene
1,8-Bis(4-hexylstyryl)pyrene
1,8-Bis(p-hexylphenylethynyl)pyrene
(1E)-1,2-Bis(4-styrylphenyl)ethene
1-((E)-2-(Pyren-3-yl)vinyl)-4-((E)-2-(pyren-8-yl)vinyl)benzene
2,3,6,7-Tetra(2-naphthyl)naphthalene
2,3,6,7-Tetra(4-biphenylyl)naphthalene
2,3,6,7-Tetraphenylnaphthalene2,3,6,7-Tetrastyrylnaphthalene
2-(4-Biphenyl)-5-(4-tert-butyl-phenyl)-1,3,4-oxadiazole
2,7-Bis(2-(4-hexylphenyl)ethynyl)pyrene
2,7-Bis(4-octylstyryl)-9,9-dimethyl-9H-fluorene
2,7-Bis(4-(trifluoromethyl)phenyl)pyrene
2,7-Bis(6-hexyl-2-naphthaleyl)-pyrene
2,9-Dimethyl-4,7-diphenyl-1,10-phenanthroline
2-(9H-Carbazol-9-yl)-5-[4'-(9H-carbazol-9-yl)-1,1'-biphenyl-4-yl]-pyridine
2-Methyl-9,10-bis(naphthalen-2-yl)anthracene
2-tert-Butyl-9,10-bis(2-naphthyl)anthracene
3,3’,5,5’-Tetraphenyl-p-terphenyl
4-(2,2-Diphenylethenyl)-N,N-bis(4-methylphenyl)Benzenamine
4,4''-(1,2-Ethenediyl)bis[4'-(butyl)-1,1'-biphenyl]
4,4''-(1,2-Ethenediyl)bis[4'-trifluoromethyl-1,1'-biphenyl]
4,4'-(1,2-Ethenediyl)bisbenzonitrile
4,4''-[1,4-Phenylenedi-(1E)-1,2-ethenediyl]bis[4'-trifluoromethyl-1,1'-biphenyl
4,4''-[1,4-Phenylenedi-(1E)-2,1-ethenediyl]bis[4'-pentyl-1,1'-bi-phenyl]
4,4'-(1,4-Phenylenedi-2,1-ethenediyl)bisbenzonitrile
4,4',4''-Tris(N-3-methylphenyl-N-phenylamino)triphenylamine
4,4’-Bis[1-(3,6,8-triphenyl)pyrenyl]biphenyl
4,4'-Bis[(1E)-2-[4'-(trifluoromet-hyl)[1,1'-biphenyl]-4-yl]ethenyl]-1,1'-biphenyl
4,4'-Bis[2-(4'-butyl[1,1'-biphenyl]-4-yl)ethenyl]-1,1'-biphenyl
4,4'-Bis[2-(4-cyclohexylphenyl)ethenyl]-1,1'-biphenyl
4,4'-Bis[2-(4-decylphenyl)ethenyl]-1,1'-biphenyl
4,4'-Bis[2-(4-dodecylphenyl)ethenyl]-1,1'-biphenyl
4,4''-Bis[2-(4-hexylphenyl)ethenyl]-1,1':4',1''-terphenyl
4,4'-Bis[2-[4-(octyloxy)phenyl]ethenyl]-1,1'-biphenyl
4,4''-Bis[2-(4-octylphenyl)ethenyl]-1,1':4',1''-terphenyl
4,4'-Bis[2-(4-octylphenyl)ethenyl]-1,1'-biphenyl
4,4''-Bis[2-(4-pentylphenyl)ethenyl]-1,1':4',1''-terphenyl
4,4'-Bis[2-(4-pentylphenyl)ethenyl]-1,1'-biphenyl
4,4'-Bis[4-(di-p-tolylamino)styryl]biphenyl
4,4'-Bis(4'-n-heptyl-4-biphenylyl)-stilbene (7CI)
4,4'-Bis(9-carbazolyl)-2,2'-dimeth-ylbiphenyl
4,4’-Bis[di(m-tolyl)amino]terphenyl
4,4’-Bis(diphenylamino)terphenyl
4',4''-Bis[di(p-tert-butylphenyl)amino]-p-terphenyl
4,4'-Bis(N-carbazolyl)-1,1'-biphenyl
4,7-Diphenyl-1,10-phenanthroline
5,5'-Bis[1-(3,6,8-triphenyl)pyrenyl]-2,2'-bipydine
7,7'-Spirobi[7H-dinaphtho[2,1-b:1',2'-d]silole] (9CI)
7,12-Diphenylbenzo[k]fluoranthene
9-(3-(4-(3,5-Bis(9H-carbazol-9-yl)styryl)styryl)-5-(9H-carbazol-9-yl)phenyl)-9H-carbazole
9-(4-(4-(4-(9H-Carbazol-9-yl)styryl)styryl)phenyl)-9H-carbazole
9,9'-[[1,1'-Biphenyl]-4,4'-diylbis-(2,1-ethenediyl-3,1-phenylene)]bis-9H-carbazole
9,9'-(1,6-Pyrenediyldi-4,1-phenylene)bis-9H-Carbazole
9,9'-(2,6-Pyridinediyl)bis-9H-carbazole
9,9',9'',9'''-[[1,1'-Biphenyl]-4,4'-diylbis(2,1-ethenediyl-5,1,3-benzenetriyl)]tetrakis-9H-carbazole
9,9'-Biphenyl-3,3'-diylbis-9H-carbazole
9,9-Bis[4-[N,N'-di(4-biphenylyl)amino]phenyl]fluorene
9,10-Bis([1,1'-biphenyl]-3-yl)anthracene
9,10-Diphenylanthracene
a,a'-(1,4-Phenylenedimethylidyne)bis-4-ethyl-benzeneacetonitrile
a,a'-Bis(4-ethyl-phenylmethylene)-1,4-benzenediacetonitrile
Bis[2-(diphenylphosphino)phenyl]ether oxide
Cupper(II) phthalocyanine
Dioctylbenzothieno[2,3-b]benzothiophene
Dipyrazino[2,3-f:2',3'-h]quinoxaline-2,3,6,7,10,11-hexacarbonitrile
Fullerene C60
N4-[4'-(Diphenylamino)-[3,3'-dimethyl-1,1'-biphenyl]-4-yl]-N4,N4',N4'-triphenyl-[3,3'-dime-thyl-1,1'-biphenyl]-4,4'-diamine
N4,N4''-(9H-Fluoren-9-ylidenedi-4,1-phenylene)bis[N4,N4',N4'-triphenyl-[1,1'-biphenyl]-4,4'-diamine]
N4,N4'-Bis[4'-([1,1'-biphenyl]-3-ylphenylamino)[1,1'-biphenyl]-4-yl]-N4,N4'-diphenyl-[1,1'-biphenyl]-4,4'-diamine
N4,N4'-Bis[4'-[(4-tert-butylphenyl)phenylamino][1,1'-biphenyl]-4-yl]-N4,N4'-diphenyl[1,1'-biphenyl]-4,4'-diamine
N4,N4'-(Biphenyl-4,4'-diyl)bis(N4,N4',N4'-triphenylbiphenyl-4,4'diamine)
N4,N4''-Bis[4'-(diphenylamino)[1,1'-biphenyl]-4-yl]-N4,N4''-diphenyl-[1,1':4',1''-terphenyl]-4,4''-diamine
N4,N4''-(Cyclohexylidenedi-4,1-phenylene)bis[N4,N4',N4'-triphenyl-[1,1'-biphenyl]-4,4'-diamine]
N4,N4,N4',N4'-Tetra([1,1'-biphenyl]-3-yl)[1,1'-biphenyl]-4,4'-diamine
Naphtho[2,3-b]naphtho[2',3':4,5]thieno[2,3-d]thiophene
N,N'-Bis(3-methylphenyl)-N',N'-bis(phenyl)-benzidine
N,N'-Bis[4'-([1,1'-biphenyl]-4-yl-phenylamino)[1,1'-biphenyl]-4-yl]-N,N'-diphenyl[1,1':4',1''-terphenyl]-4,4''-diamine
N,N-Bis[4'-(diphenylamino)[1,1'-biphenyl]-4-yl]-N',N'-diphenyl-[1,1'-biphenyl]-4,4'-diamine
N,N'-Bis[4'-(diphenylamino)[1,1'-biphenyl-4yl]-N,N'diphenyl-[3-phenyl-1,1'-biphenyl]-4,4'-diamine
N,N'-Di(1-naphthyl)-N,N'-diphenylbenzidine
N,N'-Diphenyl-N,N'-di-[4-(N,N-ditolyl-amino)phenyl]benzidine
N,N,N',N'-Tetra(4-biphenylyl)benzidine
PentacenePhenyl-dipyreylphosphine oxide
Tris(8-hydroxyquinolinato)aluminium
略称材料名索引
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